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"Primary use for the reactor is cellulose derivatization. The cellulose material to be mixed is mainly moist, sticky and fibrous, and the reactions will be done in high consistencies. \u201cHigh-consistency\u201d refers to cellulose pulp, which contains even less than 70% water. At this consistency, the pulp behaves almost like a solid and is challenging to mix. Thus special mixing elements such as shovels and chopper(s) are required. Mixing shovels are to enable complete mixing throughout the whole reactor volume, such as ploughshare shovels. Chopper is required to shred the cellulose material and ensure homogenous mixing conditions and that the mixed material is not only rotated around the reactor. The mixing elements should be able to disperse cellulose fibers but the mixing should not be so strong that it breaks the individual fibers. This is important when the desired product is surface-treated cellulose fibers, as opposed to \u201cbulk treated\u201d cellulose, where the entire cellulose fiber structure is derivatized. Our goal is to be able to do both surface-treatments and bulk treatments.",
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"\u2022\tThe cellulose pulp is mixed with additives, the reactor is heated to a desired temperature, derivatizing reagents are added, and the reaction is allowed to proceed.",
"\u2022\tThe main reaction solvent is tap water.",
"\u2022\tHeating is achieved by feeding steam into a jacket, which is around the reactor drum. In this document, the term \u201creactor drum\u201d refers to the part of the reactor where the mixing and reactions take place. For reactions that require higher pressures than what the solvent\u2019s vapor pressure naturally induces in a given temperature, pressurized air will be used to increase the pressure in the drum. In exothermic reactions, the temperature might need to be lowered by feeding cold water into the jacket.",
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"\u2022\tReactor volume minimum 100 liters",
"\u2022\tThe operational gauge pressure range of the reactor at least 0-10 bar",
"\u2022\tThe operational temperature range at least 0-180\u00b0C",
"\u2022\tAll rotating connections equipped with double mechanical seal",
"\u2022\tInclude minimum one chopper or similar homogenizing element(s)",
"\u2022\tDischarge valves must be operated by hydraulic, pneumatic, electric etc. non-manual means",
"\u2022\tDead volume of the discharge valve system should be minimized",
"\u2022\tFeed and discharge valves must be equipped with safety device, which prevents opening while vessel is pressurized",
"\u2022\tFor emptying and flushing purposes the main drive must be able to rotate while feed and discharge valves are open",
"\u2022\tThe discharge valve must be located in the bottom of the reactor. Minimum distance between lowest point of discharge valve system and floor is 800 mm. This is not required if the reactor can be tilted to allow for draining of product efficiently",
"\u2022\tMain drive and choppers motors controlled by frequency converter and adjustable via user interface",
"\u2022\tMain drive power minimum 10 kW",
"\u2022\tMain drive rotation speed minimum 150 rpm",
"\u2022\tChopper motor power minimum 5 kW",
"\u2022\tChopper rotation speed minimum 2 500 rpm",
"\u2022\tReactor drum, mixing element and heating jacket material AISI 316 L (1.4404)",
"\u2022\tReactor is heated with steam and cooled with water. Steam generation unit is not included in the scope of supply. However, the heating\/cooling jacket (all, if consists of multiple parts) must have connections at the lowest and highest point of the jacket",
"\u2022\tMixer is to include connection flanges that enable minimum five (5) connections for reagents and\/or measurements",
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"\u2022\tEquipment will be placed in non-ATEX area. Equipment does not need to be ATEX compatible.",
"\u2022\tReactions will be done in mostly aqueous media.",
"\u2022\tA used device is also acceptable if it fulfills the set criteria."
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